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Direct fluorescence detection of Pb^<2+> and Cd^<2+> by high performance liquid chromatography using 1-(4-Aminobenzyl)ethylenediamine-N,N,N’,N’-tetraacetate as a pre-column derivatizing agent
https://sucra.repo.nii.ac.jp/records/13137
https://sucra.repo.nii.ac.jp/records/13137b3fab821-68d7-49f1-98a8-153fe356ab13
名前 / ファイル | ライセンス | アクション |
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A1002469.pdf (200.4 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2008-03-10 | |||||
タイトル | ||||||
タイトル | Direct fluorescence detection of Pb^<2+> and Cd^<2+> by high performance liquid chromatography using 1-(4-Aminobenzyl)ethylenediamine-N,N,N’,N’-tetraacetate as a pre-column derivatizing agent | |||||
言語 | ||||||
言語 | eng | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Lead ion | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Cadmium ion | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Aromatic polyaminocarboxylate | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Dissociation kinetics | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Pre-column derivatization | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Fluorescent detection | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | journal article | |||||
著者 |
齋藤, 伸吾
× 齋藤, 伸吾× Danzaka, Naoki× 星, 座 |
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著者 ローマ字 | ||||||
Saito, Shingo | ||||||
著者 ローマ字 | ||||||
Danzaka, Naoki | ||||||
著者 ローマ字 | ||||||
Hoshi, Suwaru | ||||||
著者 所属 | ||||||
北見工業大学工学部工学研究科環境化学講座環境分析研究室(現 : 埼玉大学大学院理工学研究科物質科学部門) | ||||||
著者 所属(別言語) | ||||||
Department of Applied and Environmental Chemistry, Kitami Institute of Technology, | ||||||
書誌情報 |
Journal of Chromatography A, 巻 1104, 号 1-2, p. 140-144, 発行日 2006 |
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年月次 | ||||||
2006-2 | ||||||
出版者名 | ||||||
出版者 | Elsevier B.V. | |||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 00219673 | |||||
DOI | ||||||
関連タイプ | isVersionOf | |||||
識別子タイプ | DOI | |||||
関連識別子 | info:doi/10.1016/j.chroma.2005.11.085 | |||||
関連サイト | ||||||
内容記述タイプ | Other | |||||
内容記述 | http://www.sciencedirect.com/science/journal/00219673 | http://www.sciencedirect.com/science/journal/00219673 | |||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | A highly sensitive HPLC with direct fluorescent detection (λex = 235 nm, λem = 355 nm) was developed for Pb^<2+> and Cd^<2+> complexes with an aromatic polyaminocarboxylate, 1-(4-aminobenzyl)ethylenediamine-N,N,N′,N′-tetraacetate as a pre-column derivatizing agent. A reversed phase partition column pretreated by a cationic surfactant was employed. Although this ligand forms thermodynamically stable complexes with various metal ions, only peaks of Pb^<2+> and Cd^<2+> were detected with the ligand-centered emission in the HPLC due to the emissive activity and kinetic stability in the dissociation reaction. The detection limits obtained were 1.5 × 10^<-8> and 3.3 × 10^<-9> mol l^<-1> for Pb^<2+> and Cd^<2+>, respectively. | |||||
版 | ||||||
[著者版] | ||||||
著者版フラグ | ||||||
出版タイプ | AM | |||||
出版タイプResource | http://purl.org/coar/version/c_ab4af688f83e57aa | |||||
資源タイプ | ||||||
内容記述タイプ | Other | |||||
内容記述 | text | |||||
フォーマット | ||||||
内容記述タイプ | Other | |||||
内容記述 | application/pdf | |||||
作成日 | ||||||
日付 | 2008-03-10 | |||||
日付タイプ | Created | |||||
アイテムID | ||||||
A1002469 |