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Characterization and Determination of Linear Alkylbenzenesulfonates in Environmental Water Samples by High-Performance Liquid Chromatography with a Hydrophilic Polymer Column and Electrospray Ionization Mass Spectrometric Detection
https://sucra.repo.nii.ac.jp/records/13160
https://sucra.repo.nii.ac.jp/records/131608f3354fe-94da-417e-b1af-8225a228f76e
名前 / ファイル | ライセンス | アクション |
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A1002484.pdf (80.9 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2008-03-12 | |||||
タイトル | ||||||
タイトル | Characterization and Determination of Linear Alkylbenzenesulfonates in Environmental Water Samples by High-Performance Liquid Chromatography with a Hydrophilic Polymer Column and Electrospray Ionization Mass Spectrometric Detection | |||||
言語 | ||||||
言語 | eng | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | journal article | |||||
著者 |
NISHIGAKI, Atsuko
× NISHIGAKI, Atsuko× KUROIWA, Chiaki× 渋川, 雅美 |
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著者 ローマ字 | ||||||
NISHIGAKI, Atsuko | ||||||
著者 ローマ字 | ||||||
KUROIWA, Chiaki | ||||||
著者 ローマ字 | ||||||
SHIBUKAWA, Masami | ||||||
著者 所属 | ||||||
著者 所属 | ||||||
著者 所属 | ||||||
日本大学生産工学部応用分子化学科 | ||||||
著者 所属(別言語) | ||||||
著者 所属(別言語) | ||||||
著者 所属(別言語) | ||||||
Department of Applied Molecular Chemistry, College of Industrial Technology, Nihon University | ||||||
書誌情報 |
Analytical Sciences 巻 20, 号 1, p. 143-147, 発行日 2004 |
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年月次 | ||||||
2004-1 | ||||||
出版者名 | ||||||
出版者 | The Japan Society for Analytical Chemistry | |||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 09106340 | |||||
DOI | ||||||
関連タイプ | isIdenticalTo | |||||
識別子タイプ | DOI | |||||
関連識別子 | info:doi/10.2116/analsci.20.143 | |||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | A liquid chromatography-mass spectrometry (LC/MS) method was developed for the separation and determination of linear alkylbenzenesulfonates (C10 - C14 LAS) in environmental water samples using a hydrophilic polymer column (Shodex Mspak GF-310 4D). This method involves a solid-phase extraction of the LAS samples with a Sep-Pak PS-2 cartridge. The LAS components were separated on the column with a mobile phase of 29% (w/v) acetonitrile-water containing 0.8 mM di-n-butylammonium acetate and 0.2 M acetic acid, and were detected by mass spectrometry with electrospray ionization. Detection limits of the developed method based on selected ion monitoring (SIM) technique for the C10 - C14 LAS standards were 13 - 47 ng L-1. The concentrations of the C10 - C14 LAS in the environmental water samples ranged between 5 - 317 μg L-1 for a river water sample and 0.4 - 6.4 μg L-1 for a seawater sample. Linear relationships between the logarithms of retention factors and the alkyl chain lengths for each phenyl positional isomer of LAS could successfully be used for the identification of the isomer peaks. | |||||
版 | ||||||
[出版社版] | ||||||
著者版フラグ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
資源タイプ | ||||||
内容記述タイプ | Other | |||||
内容記述 | text | |||||
フォーマット | ||||||
内容記述タイプ | Other | |||||
内容記述 | application/pdf | |||||
作成日 | ||||||
日付 | 2008-03-11 | |||||
日付タイプ | Created | |||||
アイテムID | ||||||
A1002484 |