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ゾル-ゲル法によるZrSiO_4粉末の合成(第1報) : 出発原料及び種子結晶添加の影響
https://sucra.repo.nii.ac.jp/records/13006
https://sucra.repo.nii.ac.jp/records/13006ba082b6e-77c1-4511-bed7-74a63aed129a
名前 / ファイル | ライセンス | アクション |
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A1002255.pdf (538.5 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2008-01-09 | |||||
タイトル | ||||||
タイトル | ゾル-ゲル法によるZrSiO_4粉末の合成(第1報) : 出発原料及び種子結晶添加の影響 | |||||
言語 | ||||||
言語 | jpn | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | ZrSiO_4 powder | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Sol-gel process | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Two-stage heating | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | ZrSiO_4 seeding | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | journal article | |||||
タイトル(別言語) | ||||||
その他のタイトル | Preparation of ZrSiO_4 Powder Using Sol-Gel Process (Part 1) : Influence of Starting Materials and Seeding | |||||
著者 |
小林, 秀彦
× 小林, 秀彦× 高野, 俊行× 森, 利之× 山村, 博× 三田村, 孝 |
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著者 ローマ字 | ||||||
KOBAYASHI, Hidehiko | ||||||
著者 ローマ字 | ||||||
TAKANO, Toshiyuki | ||||||
著者 ローマ字 | ||||||
MORI, Toshiyuki | ||||||
著者 ローマ字 | ||||||
YAMAMURA, Hiroshi | ||||||
著者 ローマ字 | ||||||
MITAMURA, Takashi | ||||||
著者 所属 | ||||||
埼玉大学大学院理工学研究科物質科学部門 | ||||||
著者 所属 | ||||||
埼玉大学工学部応用化学科 | ||||||
著者 所属 | ||||||
東ソー(株)新材料研究所 | ||||||
著者 所属 | ||||||
東ソー(株)新材料研究所 | ||||||
著者 所属 | ||||||
埼玉大学工学部 | ||||||
著者 所属(別言語) | ||||||
Department of Applied Chemistry, Faculty of Engineering, Saitama University | ||||||
著者 所属(別言語) | ||||||
Department of Applied Chemistry, Faculty of Engineering. Saitama University | ||||||
著者 所属(別言語) | ||||||
Advanced Materials Research Laboratory, TOSOH Co., Ltd. | ||||||
著者 所属(別言語) | ||||||
Advanced Materials Research Laboratory, TOSOH Co., Ltd. | ||||||
著者 所属(別言語) | ||||||
Department of Applied Chemistry, Faculty of Engineering. Saitama University | ||||||
書誌情報 |
日本セラミックス協会学術論文誌 巻 98, 号 1138, p. 567-572, 発行日 1990 |
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年月次 | ||||||
1990-6 | ||||||
出版者名 | ||||||
出版者 | 社団法人日本セラミックス協会 | |||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 09145400 | |||||
関連サイト | ||||||
内容記述タイプ | Other | |||||
内容記述 | http://ci.nii.ac.jp/naid/110002289078/ | http://ci.nii.ac.jp/naid/110002289078/ | |||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | The effect of temperature, heating rate and addition of ZrSiO_4 seed crystals on the preparation of ZrSiO_4 powders by the sol-gel process was studied using X-ray powder diffractometry. ZrSiO_4 powders have been prepared by different precursors in Zr(OPr^i)_4-Si(OEt)_4, Zr(OPr^i)_4-SiO_2 sol, ZrOCL_2・8 H_2O-Si(OEt)_4 and ZrOCl_2・8H_2O-SiO_2 sol groups. The formation rate of ZrSiO_4 was higher in Si(OEt)_4 than in SiO_2 sol. The formation rate was influenced by heating rate, and, in particular, increased remarkably below 2.5 K/min. When a small amount of commercial ZrSiO_4 was added to the powder of precursor composition as seed crystals, ZrSiO_4 powder with a purity of 94-96% was formed at 1600°-1650℃. It was found that the addition of seeds results in lowering of the formation temperature of ZrSiO_4 by about 100℃. On the other hand, a ZrSiO_4 powder of 94-96% purity was obtained by heating the powder of precursor composition at 1300°-1350℃ for 1 h, followed by re-heating at 1600℃ for 1 h. The results have suggested that the preparation of ZrSiO_4, powder of nearly single phase is possible using the sol-gel process by controlling the seeding and/or the two-stage heating. | |||||
注記 | ||||||
内容記述タイプ | Other | |||||
内容記述 | rights: 社団法人日本セラミックス協会 rights: 本文データは学協会の許諾に基づきCiNiiから複製したものである relation: IsVersionOf: http://ci.nii.ac.jp/naid/110002289078/ |
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版 | ||||||
[出版社版] | ||||||
著者版フラグ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
資源タイプ | ||||||
内容記述タイプ | Other | |||||
内容記述 | text | |||||
フォーマット | ||||||
内容記述タイプ | Other | |||||
内容記述 | application/pdf | |||||
作成日 | ||||||
日付 | 2008-01-09 | |||||
日付タイプ | Created | |||||
アイテムID | ||||||
A1002255 |