WEKO3
アイテム
{"_buckets": {"deposit": "7530c92b-e2b1-46e8-8820-aca7ae1d5851"}, "_deposit": {"created_by": 3, "id": "13150", "owners": [3], "pid": {"revision_id": 0, "type": "depid", "value": "13150"}, "status": "published"}, "_oai": {"id": "oai:sucra.repo.nii.ac.jp:00013150", "sets": ["426"]}, "author_link": ["21113", "21114", "21117", "21115", "18528", "21116"], "item_119_alternative_title_1": {"attribute_name": "タイトル(別言語)", "attribute_value_mlt": [{"subitem_alternative_title": "Visual fluorimetry of trace lead using ion-pair extraction onto an octadecylsilanized silica disk"}]}, "item_119_biblio_info_8": {"attribute_name": "書誌情報", "attribute_value_mlt": [{"bibliographicIssueDates": {"bibliographicIssueDate": "2002", "bibliographicIssueDateType": "Issued"}, "bibliographicIssueNumber": "11", "bibliographicPageEnd": "1040", "bibliographicPageStart": "1037", "bibliographicVolumeNumber": "51", "bibliographic_titles": [{"bibliographic_title": "分析化学"}]}]}, "item_119_date_31": {"attribute_name": "作成日", "attribute_value_mlt": [{"subitem_date_issued_datetime": "2008-03-11", "subitem_date_issued_type": "Created"}]}, "item_119_description_19": {"attribute_name": "抄録", "attribute_value_mlt": [{"subitem_description": "A rapid and simple method has been developed for the determination of trace lead ion using an octadecylsilanized (ODS) silica disk cartridge. The ion-pair of a lead complex with 5,6-14,15-dibenzo-4,7,13,16,21,24-hexaoxa-1.10-diazabicyclohexacosane (DBC 2.2.2) and tetrabromofluorescein (Eosin Y) was extracted from a sample solution onto an ODS filter at pH7.0. It was found that the addition of 20 wt% ethanol to the sample solution significantly enhanced the solid phase extraction. The lead concentration was determined by visual fluorimetry under ultraviolet light in the dark. The ion-pair has excitation and emission maxima at 530 nm and 560 nm in the solid phase, respectively. When measured with a densitometer, the linear range of this method is up to 2.9×10^-8 mol dm^-3(6 ppb). The detection limit is 5.0×10^-10 mol dm^-3 (100 ppt) by visual determination and 3.4×10^-9 mol dm^-3 (700 ppt) by densitometry. The relative standard deviation for 1.2×10^-3 mol dm^-3 (2.3 ppb) of lead is 5.6% (n=7). The method is essentially free from matrix interference. The proposed method can easily be performed and provides good precision and accuracy.", "subitem_description_type": "Abstract"}]}, "item_119_description_29": {"attribute_name": "資源タイプ", "attribute_value_mlt": [{"subitem_description": "text", "subitem_description_type": "Other"}]}, "item_119_description_30": {"attribute_name": "フォーマット", "attribute_value_mlt": [{"subitem_description": "application/pdf", "subitem_description_type": "Other"}]}, "item_119_other_language_22": {"attribute_name": "その他の言語", "attribute_value_mlt": [{"subitem_language": "eng"}]}, "item_119_publisher_11": {"attribute_name": "出版者名", "attribute_value_mlt": [{"subitem_publisher": "社団法人日本分析化学会"}]}, "item_119_relation_7": {"attribute_name": "著者 外部リンク", "attribute_value_mlt": [{"subitem_relation_name": [{"subitem_relation_name_text": "\u0026EMPTY\u0026"}], "subitem_relation_type_id": {"subitem_relation_type_id_text": "\u0026EMPTY\u0026", "subitem_relation_type_select": "URI"}}, {"subitem_relation_name": [{"subitem_relation_name_text": "\u0026EMPTY\u0026"}], "subitem_relation_type_id": {"subitem_relation_type_id_text": "\u0026EMPTY\u0026", "subitem_relation_type_select": "URI"}}, {"subitem_relation_name": [{"subitem_relation_name_text": "\u0026EMPTY\u0026"}], "subitem_relation_type_id": {"subitem_relation_type_id_text": "\u0026EMPTY\u0026", "subitem_relation_type_select": "URI"}}, {"subitem_relation_name": [{"subitem_relation_name_text": "http://s-read.saitama-u.ac.jp/researchers/pages/researcher/lZwKkNhN"}], "subitem_relation_type_id": {"subitem_relation_type_id_text": "http://s-read.saitama-u.ac.jp/researchers/pages/researcher/lZwKkNhN", "subitem_relation_type_select": "URI"}}]}, "item_119_source_id_14": {"attribute_name": "ISSN", "attribute_value_mlt": [{"subitem_source_identifier": "05251931", "subitem_source_identifier_type": "ISSN"}]}, "item_119_text_27": {"attribute_name": "版", "attribute_value_mlt": [{"subitem_text_value": "[出版社版]"}]}, "item_119_text_3": {"attribute_name": "著者 ローマ字", "attribute_value_mlt": [{"subitem_text_value": "ISOE, Junichi"}, {"subitem_text_value": "SAKAI, Yasuhiro"}, {"subitem_text_value": "KANEKO, Emiko"}, {"subitem_text_value": "SAITO, Shingo"}, {"subitem_text_value": "HOSHI, Suwaru"}, {"subitem_text_value": "AKATSUKA, Kunihiko"}]}, "item_119_text_32": {"attribute_name": "アイテムID", "attribute_value_mlt": [{"subitem_text_value": "A1002493"}]}, "item_119_text_35": {"attribute_name": "公開日(XooNIps)", "attribute_value_mlt": [{"subitem_text_value": "Mar 12, 2008 09:00:00"}]}, "item_119_text_36": {"attribute_name": "最終更新日(XooNIps)", "attribute_value_mlt": [{"subitem_text_value": "Sep 8, 2009 11:04:40"}]}, "item_119_text_37": {"attribute_name": "更新履歴(XooNIps)", "attribute_value_mlt": [{"subitem_text_value": "Sep 8, 2009 フリーキーワード, 著者 を変更"}, {"subitem_text_value": "Mar 18, 2009 フリーキーワード, キーワード, 言語 を変更"}, {"subitem_text_value": "Mar 18, 2009 フリーキーワード, キーワード, 言語 を変更"}, {"subitem_text_value": "Oct 11, 2008 フリーキーワード, インデックス, キーワード, 言語 を変更"}, {"subitem_text_value": "Mar 31, 2008 フリーキーワード, キーワード, 言語 を変更"}, {"subitem_text_value": "Mar 31, 2008 フリーキーワード, キーワード, 言語 を変更"}, {"subitem_text_value": "Mar 26, 2008 フリーキーワード, キーワード, 言語 を変更"}, {"subitem_text_value": "Mar 26, 2008 フリーキーワード, キーワード, 言語 を変更"}, {"subitem_text_value": "Mar 12, 2008 フリーキーワード, インデックス, キーワード, 言語 を変更"}, {"subitem_text_value": "Mar 12, 2008 ID, フリーキーワード, インデックス, 版, キーワード, 言語 を変更"}]}, "item_119_text_38": {"attribute_name": "登録者(XooNIps)", "attribute_value_mlt": [{"subitem_text_value": "sucra_jim4"}]}, "item_119_text_39": {"attribute_name": "閲覧数(XooNIps)", "attribute_value_mlt": [{"subitem_text_value": "1291"}]}, "item_119_text_4": {"attribute_name": "著者 所属", "attribute_value_mlt": [{"subitem_text_value": "北見工業大学大学院工学研究科"}, {"subitem_text_value": "東北大学大学院工学研究科[現: シスメックス(株)]"}, {"subitem_text_value": "北見工業大学大学院工学研究科"}, {"subitem_text_value": "北見工業大学大学院工学研究科[現: 埼玉大学大学院理工学研究科]"}, {"subitem_text_value": "北見工業大学大学院工学研究科"}, {"subitem_text_value": "北見工業大学大学院工学研究科"}]}, "item_119_text_40": {"attribute_name": "ダウンロード数(XooNIps)", "attribute_value_mlt": [{"subitem_text_value": "452"}]}, "item_119_text_41": {"attribute_name": "XooNIps_インデックス", "attribute_value_mlt": [{"subitem_text_value": "sucra_jim4|Public/埼玉大学/理工学研究科|Public/埼玉大学/理工学研究科/物質科学部門|Public/主題別/化学/複合化学/分析化学|Public/ジャンル別/学術雑誌論文(国内)/日本分析化学会"}]}, "item_119_text_42": {"attribute_name": "XooNIps_ITEM_KEY", "attribute_value_mlt": [{"subitem_text_value": "2028"}]}, "item_119_text_5": {"attribute_name": "著者 所属(別言語)", "attribute_value_mlt": [{"subitem_text_value": "Department of Applied and Environmental Chemistry, Graduate School of Engineering, Kitami Institute of Technology"}, {"subitem_text_value": "Department of Applied Chemistry, Graduate School of Engineering, Tohoku University[Present address: Sysmex Corporation]"}, {"subitem_text_value": "Department of Applied and Environmental Chemistry, Graduate School of Engineering, Kitami Institute of Technology"}, {"subitem_text_value": "Department of Applied and Environmental Chemistry, Graduate School of Engineering, Kitami Institute of Technology"}, {"subitem_text_value": "Department of Applied and Environmental Chemistry, Graduate School of Engineering, Kitami Institute of Technology"}, {"subitem_text_value": "Department of Applied and Environmental Chemistry, Graduate School of Engineering, Kitami Institute of Technology"}]}, "item_119_text_9": {"attribute_name": "年月次", "attribute_value_mlt": [{"subitem_text_value": "2002-11"}]}, "item_119_version_type_28": {"attribute_name": "著者版フラグ", "attribute_value_mlt": [{"subitem_version_resource": "http://purl.org/coar/version/c_970fb48d4fbd8a85", "subitem_version_type": "VoR"}]}, "item_creator": {"attribute_name": "著者", "attribute_type": "creator", "attribute_value_mlt": [{"creatorNames": [{"creatorName": "磯江, 準一"}], "nameIdentifiers": [{"nameIdentifier": "21113", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "酒井, 康裕"}], "nameIdentifiers": [{"nameIdentifier": "21114", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "金子, 恵美子"}], "nameIdentifiers": [{"nameIdentifier": "21115", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "齋藤, 伸吾"}, {"creatorName": "サイトウ, シンゴ", "creatorNameLang": "ja-Kana"}], "nameIdentifiers": [{"nameIdentifier": "18528", "nameIdentifierScheme": "WEKO"}, {"nameIdentifier": "lZwKkNhN", "nameIdentifierScheme": "研究者総覧", "nameIdentifierURI": "http://s-read.saitama-u.ac.jp/researchers/pages/researcher/lZwKkNhN"}]}, {"creatorNames": [{"creatorName": "星, 座"}], "nameIdentifiers": [{"nameIdentifier": "21116", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "赤塚, 邦彦"}], "nameIdentifiers": [{"nameIdentifier": "21117", "nameIdentifierScheme": "WEKO"}]}]}, "item_files": {"attribute_name": "ファイル情報", "attribute_type": "file", "attribute_value_mlt": [{"accessrole": "open_date", "date": [{"dateType": "Available", "dateValue": "2018-01-24"}], "displaytype": "detail", "download_preview_message": "", "file_order": 0, "filename": "A1002493.pdf", "filesize": [{"value": "320.9 kB"}], "format": "application/pdf", "future_date_message": "", "is_thumbnail": false, "licensetype": "license_free", "mimetype": "application/pdf", "size": 320900.0, "url": {"label": "A1002493.pdf", "url": "https://sucra.repo.nii.ac.jp/record/13150/files/A1002493.pdf"}, "version_id": "7f6d2293-1fc6-4017-b987-c40a24ab0557"}]}, "item_keyword": {"attribute_name": "キーワード", "attribute_value_mlt": [{"subitem_subject": "lead", "subitem_subject_scheme": "Other"}, {"subitem_subject": "visual fluorimetry", "subitem_subject_scheme": "Other"}, {"subitem_subject": "ion-pair extraction", "subitem_subject_scheme": "Other"}, {"subitem_subject": "ODS disk", "subitem_subject_scheme": "Other"}, {"subitem_subject": "DBC 2.2.2", "subitem_subject_scheme": "Other"}, {"subitem_subject": "Eosin Y", "subitem_subject_scheme": "Other"}]}, "item_language": {"attribute_name": "言語", "attribute_value_mlt": [{"subitem_language": "jpn"}]}, "item_resource_type": {"attribute_name": "資源タイプ", "attribute_value_mlt": [{"resourcetype": "journal article", "resourceuri": "http://purl.org/coar/resource_type/c_6501"}]}, "item_title": "オクタデシルシリル化シリカディスクを用いる微量鉛のイオン対抽出/蛍光目視定量", "item_titles": {"attribute_name": "タイトル", "attribute_value_mlt": [{"subitem_title": "オクタデシルシリル化シリカディスクを用いる微量鉛のイオン対抽出/蛍光目視定量"}]}, "item_type_id": "119", "owner": "3", "path": ["426"], "permalink_uri": "https://sucra.repo.nii.ac.jp/records/13150", "pubdate": {"attribute_name": "公開日", "attribute_value": "2008-03-12"}, "publish_date": "2008-03-12", "publish_status": "0", "recid": "13150", "relation": {}, "relation_version_is_last": true, "title": ["オクタデシルシリル化シリカディスクを用いる微量鉛のイオン対抽出/蛍光目視定量"], "weko_shared_id": -1}
オクタデシルシリル化シリカディスクを用いる微量鉛のイオン対抽出/蛍光目視定量
https://sucra.repo.nii.ac.jp/records/13150
https://sucra.repo.nii.ac.jp/records/13150e8eb5621-6331-4534-9923-f9cf57522eed
名前 / ファイル | ライセンス | アクション |
---|---|---|
A1002493.pdf (320.9 kB)
|
|
Item type | 学術雑誌論文 / Journal Article(1) | |||||
---|---|---|---|---|---|---|
公開日 | 2008-03-12 | |||||
タイトル | ||||||
タイトル | オクタデシルシリル化シリカディスクを用いる微量鉛のイオン対抽出/蛍光目視定量 | |||||
言語 | ||||||
言語 | jpn | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | lead | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | visual fluorimetry | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | ion-pair extraction | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | ODS disk | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | DBC 2.2.2 | |||||
キーワード | ||||||
主題Scheme | Other | |||||
主題 | Eosin Y | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | journal article | |||||
タイトル(別言語) | ||||||
その他のタイトル | Visual fluorimetry of trace lead using ion-pair extraction onto an octadecylsilanized silica disk | |||||
著者 |
磯江, 準一
× 磯江, 準一× 酒井, 康裕× 金子, 恵美子× 齋藤, 伸吾× 星, 座× 赤塚, 邦彦 |
|||||
著者 ローマ字 | ||||||
ISOE, Junichi | ||||||
著者 ローマ字 | ||||||
SAKAI, Yasuhiro | ||||||
著者 ローマ字 | ||||||
KANEKO, Emiko | ||||||
著者 ローマ字 | ||||||
SAITO, Shingo | ||||||
著者 ローマ字 | ||||||
HOSHI, Suwaru | ||||||
著者 ローマ字 | ||||||
AKATSUKA, Kunihiko | ||||||
著者 所属 | ||||||
北見工業大学大学院工学研究科 | ||||||
著者 所属 | ||||||
東北大学大学院工学研究科[現: シスメックス(株)] | ||||||
著者 所属 | ||||||
北見工業大学大学院工学研究科 | ||||||
著者 所属 | ||||||
北見工業大学大学院工学研究科[現: 埼玉大学大学院理工学研究科] | ||||||
著者 所属 | ||||||
北見工業大学大学院工学研究科 | ||||||
著者 所属 | ||||||
北見工業大学大学院工学研究科 | ||||||
著者 所属(別言語) | ||||||
Department of Applied and Environmental Chemistry, Graduate School of Engineering, Kitami Institute of Technology | ||||||
著者 所属(別言語) | ||||||
Department of Applied Chemistry, Graduate School of Engineering, Tohoku University[Present address: Sysmex Corporation] | ||||||
著者 所属(別言語) | ||||||
Department of Applied and Environmental Chemistry, Graduate School of Engineering, Kitami Institute of Technology | ||||||
著者 所属(別言語) | ||||||
Department of Applied and Environmental Chemistry, Graduate School of Engineering, Kitami Institute of Technology | ||||||
著者 所属(別言語) | ||||||
Department of Applied and Environmental Chemistry, Graduate School of Engineering, Kitami Institute of Technology | ||||||
著者 所属(別言語) | ||||||
Department of Applied and Environmental Chemistry, Graduate School of Engineering, Kitami Institute of Technology | ||||||
書誌情報 |
分析化学 巻 51, 号 11, p. 1037-1040, 発行日 2002 |
|||||
年月次 | ||||||
2002-11 | ||||||
出版者名 | ||||||
出版者 | 社団法人日本分析化学会 | |||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 05251931 | |||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | A rapid and simple method has been developed for the determination of trace lead ion using an octadecylsilanized (ODS) silica disk cartridge. The ion-pair of a lead complex with 5,6-14,15-dibenzo-4,7,13,16,21,24-hexaoxa-1.10-diazabicyclohexacosane (DBC 2.2.2) and tetrabromofluorescein (Eosin Y) was extracted from a sample solution onto an ODS filter at pH7.0. It was found that the addition of 20 wt% ethanol to the sample solution significantly enhanced the solid phase extraction. The lead concentration was determined by visual fluorimetry under ultraviolet light in the dark. The ion-pair has excitation and emission maxima at 530 nm and 560 nm in the solid phase, respectively. When measured with a densitometer, the linear range of this method is up to 2.9×10^-8 mol dm^-3(6 ppb). The detection limit is 5.0×10^-10 mol dm^-3 (100 ppt) by visual determination and 3.4×10^-9 mol dm^-3 (700 ppt) by densitometry. The relative standard deviation for 1.2×10^-3 mol dm^-3 (2.3 ppb) of lead is 5.6% (n=7). The method is essentially free from matrix interference. The proposed method can easily be performed and provides good precision and accuracy. | |||||
その他の言語 | ||||||
言語 | eng | |||||
版 | ||||||
[出版社版] | ||||||
著者版フラグ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
資源タイプ | ||||||
内容記述タイプ | Other | |||||
内容記述 | text | |||||
フォーマット | ||||||
内容記述タイプ | Other | |||||
内容記述 | application/pdf | |||||
作成日 | ||||||
日付 | 2008-03-11 | |||||
日付タイプ | Created | |||||
アイテムID | ||||||
A1002493 |