{"created":"2023-05-15T15:25:23.277876+00:00","id":12998,"links":{},"metadata":{"_buckets":{"deposit":"fbd4d00b-7ddb-4b80-85bb-739fd7ee1417"},"_deposit":{"created_by":3,"id":"12998","owners":[3],"pid":{"revision_id":0,"type":"depid","value":"12998"},"status":"published"},"_oai":{"id":"oai:sucra.repo.nii.ac.jp:00012998","sets":["94:426"]},"author_link":["20706","20702","20703","20704","20701","18337","20705"],"item_119_alternative_title_1":{"attribute_name":"タイトル（別言語）","attribute_value_mlt":[{"subitem_alternative_title":"Preparation of ZrSiO_4 Powder Using Sol-Gel Process (Part 4) : Preparation from ZrOCl_2 and Colloidal SiO_2"}]},"item_119_biblio_info_8":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"1991","bibliographicIssueDateType":"Issued"},"bibliographicIssueNumber":"1147","bibliographicPageEnd":"232","bibliographicPageStart":"227","bibliographicVolumeNumber":"99","bibliographic_titles":[{"bibliographic_title":"日本セラミックス協会学術論文誌"}]}]},"item_119_date_31":{"attribute_name":"作成日","attribute_value_mlt":[{"subitem_date_issued_datetime":"2008-01-09","subitem_date_issued_type":"Created"}]},"item_119_description_17":{"attribute_name":"関連サイト","attribute_value_mlt":[{"subitem_description":"http://ci.nii.ac.jp/naid/110002291006/ | http://ci.nii.ac.jp/naid/110002291006/","subitem_description_type":"Other"}]},"item_119_description_19":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"ZrSiO_4 fine powders were prepared from zirconium oxychloride (ZrOCl_2) and colloidal silica (SiO_2). Effects of the concentration of ZrOCl_2, calcination temperature, heating rate and size of secondary particles after hydrolysis on the preparation of ZrSiO_4 fine powders have been studied. The ZrSiO_4 precursors having Zr-O-Si bond were found in all the solutions after hydrolysis, and the formation rate of ZrSi0_4 was influenced significantly by the concentration of ZrOCl_2. Also the rate in the case of other concentrations than 0.4 M was affected remarkably by heating rate, and there was a marked tendency for crystallization of ZrO_2 and SiO_2 to proceed preferentially and creation of ZrSiO_4 nucleus to be obstructed when the heating rate was slow. It is shown that ZrSiO_4 fine powders of the single phase were prepared at a relatively low temperature such as 1300℃ by forming the ZrSiO_4 precursors having Zr-O-Si bond and by controlling the secondary particle size after hydrolysis.","subitem_description_type":"Abstract"}]},"item_119_description_21":{"attribute_name":"注記","attribute_value_mlt":[{"subitem_description":"rights: 社団法人日本セラミックス協会\nrights: 本文データは学協会の許諾に基づきCiNiiから複製したものである\nrelation: IsVersionOf: http://ci.nii.ac.jp/naid/110002291006/","subitem_description_type":"Other"}]},"item_119_description_29":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"subitem_description":"text","subitem_description_type":"Other"}]},"item_119_description_30":{"attribute_name":"フォーマット","attribute_value_mlt":[{"subitem_description":"application/pdf","subitem_description_type":"Other"}]},"item_119_publisher_11":{"attribute_name":"出版者名","attribute_value_mlt":[{"subitem_publisher":"社団法人日本セラミックス協会"}]},"item_119_source_id_14":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"09145400","subitem_source_identifier_type":"ISSN"}]},"item_119_text_27":{"attribute_name":"版","attribute_value_mlt":[{"subitem_text_value":"[出版社版]"}]},"item_119_text_3":{"attribute_name":"著者 ローマ字","attribute_value_mlt":[{"subitem_text_value":"MORI, toshiyuki"},{"subitem_text_value":"HOSHINO, Hirokuni"},{"subitem_text_value":"ISHIKAWA, Yoshimitsu"},{"subitem_text_value":"YAMAGUCHI, Teiji"},{"subitem_text_value":"YAMAMURA, Hiroshi"},{"subitem_text_value":"KOBAYASHI, Hidehiko,"},{"subitem_text_value":"MITAMURA, Takashi"}]},"item_119_text_32":{"attribute_name":"アイテムID","attribute_value_mlt":[{"subitem_text_value":"A1002248"}]},"item_119_text_4":{"attribute_name":"著者 所属","attribute_value_mlt":[{"subitem_text_value":"東ソー(株)新材料研究所"},{"subitem_text_value":"東ソー(株)新材料研究所"},{"subitem_text_value":"東ソー(株)新材料研究所"},{"subitem_text_value":"東ソー(株)新材料研究所"},{"subitem_text_value":"東ソー(株)新材料研究所"},{"subitem_text_value":"埼玉大学大学院理工学研究科物質科学部門"},{"subitem_text_value":"埼玉大学工学部"}]},"item_119_text_5":{"attribute_name":"著者 所属(別言語)","attribute_value_mlt":[{"subitem_text_value":"Advanced Materials Research Laboratory, TOSHO Co., Ltd."},{"subitem_text_value":"Advanced Materials Research Laboratory, TOSHO Co., Ltd."},{"subitem_text_value":"Advanced Materials Research Laboratory, TOSHO Co., Ltd."},{"subitem_text_value":"Advanced Materials Research Laboratory, TOSHO Co., Ltd."},{"subitem_text_value":"Advanced Materials Research Laboratory, TOSHO Co., Ltd."},{"subitem_text_value":"Department of Applied Chemistry, Faculty of Engineering, Saitama University"},{"subitem_text_value":"Faculty of Engineering, Saitama University"}]},"item_119_text_9":{"attribute_name":"年月次","attribute_value_mlt":[{"subitem_text_value":"1991-3"}]},"item_119_version_type_28":{"attribute_name":"著者版フラグ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_970fb48d4fbd8a85","subitem_version_type":"VoR"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"森, 利之"},{"creatorName":"モリ, トシユキ","creatorNameLang":"ja-Kana"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"星野, 浩邦"},{"creatorName":"ホシノ, ヒロクニ","creatorNameLang":"ja-Kana"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"石川, 芳光"},{"creatorName":"イシカワ, ヨシミツ","creatorNameLang":"ja-Kana"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"山口, 禎二"},{"creatorName":"ヤマグチ, テイジ","creatorNameLang":"ja-Kana"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"山村, 博"},{"creatorName":"ヤマムラ, ヒロシ","creatorNameLang":"ja-Kana"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"小林, 秀彦"},{"creatorName":"コバヤシ, ヒデヒコ","creatorNameLang":"ja-Kana"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"三田村, 孝"},{"creatorName":"ミタムラタカシ","creatorNameLang":"ja-Kana"}],"nameIdentifiers":[{}]}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2018-01-24"}],"displaytype":"detail","filename":"A1002248.pdf","filesize":[{"value":"1.0 MB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"label":"A1002248.pdf","url":"https://sucra.repo.nii.ac.jp/record/12998/files/A1002248.pdf"},"version_id":"da0a8c45-c984-4351-be77-c2973d1a92d8"}]},"item_keyword":{"attribute_name":"キーワード","attribute_value_mlt":[{"subitem_subject":"Sol-gel process","subitem_subject_scheme":"Other"},{"subitem_subject":"ZrSiO_4 powder","subitem_subject_scheme":"Other"},{"subitem_subject":"ZrOCl_2","subitem_subject_scheme":"Other"},{"subitem_subject":"Colloidal SiO_2","subitem_subject_scheme":"Other"},{"subitem_subject":"Hydrolysis","subitem_subject_scheme":"Other"},{"subitem_subject":"ZrSiO_4 precursor","subitem_subject_scheme":"Other"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"jpn"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"journal article","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"ゾル-ゲル法によるZrSiO_4粉末の合成(第4報) : ZrOCl_2とコロイダルSiO_2からの合成","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"ゾル-ゲル法によるZrSiO_4粉末の合成(第4報) : ZrOCl_2とコロイダルSiO_2からの合成"}]},"item_type_id":"119","owner":"3","path":["426"],"pubdate":{"attribute_name":"公開日","attribute_value":"2008-01-09"},"publish_date":"2008-01-09","publish_status":"0","recid":"12998","relation_version_is_last":true,"title":["ゾル-ゲル法によるZrSiO_4粉末の合成(第4報) : ZrOCl_2とコロイダルSiO_2からの合成"],"weko_creator_id":"3","weko_shared_id":-1},"updated":"2023-05-16T12:44:16.331583+00:00"}